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Tag : Ketal Ester

Multi-step Synthesis of Ketal Ester

Written by Jimmy Table of 1H NMR Spectral Data of Ketal ester  Table of 13C NMR Spectral Data of Ketal ester        Table of IR Spectral Data of Ketal ester   Provide your experimental index of refraction and correction factor: 1.4229 @ 22ºC 1.4229+0.00045*2=1.4238   Literature=1.4377   Reproduce your Theoretical and Percent Yield Calculations. Ethyl Acetoacetate: 10.0 mL (1.029g/mL) (1/130.14g/mol) = 0.0791 mol Glycol:  4.5 mL (1.113g/mL) (1/62.07g/mol) = 0.0807 mol 1:1 ratio of prods to reacts and reacts […]