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Synthesis of 4-bromochalcone & 3-(4-bromophenyl)-5-phenylisoxazole

Synthesis of 4-bromochalcone & 3-(4-bromophenyl)-5-phenylisoxazole

Appendix #3

IR_4-bromochalcone
Figure 18: IR spectrum of 4-bromochalcone

Integation 2 1 9
NMR-4-bromochalcone
Figure 19: Proton NMR of 4-bromochalcone

Carbon-13-NMR-4-bromochalcone
Figure 20: Carbon-13 NMR of 4-bromochalcone

DEPT-45-4-bromochalcone
Figure 21: DEPT 45 of 4-bromochalcone

DEPT-90-4-bromochalcone
Figure 22: DEPT 90 of 4-bromochalcone

DEPT-135-4-bromochalcone
Figure 23: DEPT 135 of 4-bromochalcone

COSY_4-bromochalcone
Figure 24: COSY of 4-bromochalcone

HETCOR_4-bromochalcone
Figure 25: HETCOR of 4-bromochalcone

Mass_Spec_4-bromochalcone
Figure 26: Mass Spectrum of 4-bromochalcone with match from spectral library

Appendix #4

NMR_product
Figure 27: Proton NMR of 2,3-dibromo-3-(4-bromophenyl)-1-phenylpropan-1-one

Carbon_13_NMR_product
Figure 28: Carbon-13 Spectrum of 2,3-dibromo-3-(4-bromophenyl)-1-phenylpropan-1-one

DEPT_45_product
Figure 29: DEPT 45 of 2,3-dibromo-3-(4-bromophenyl)-1-phenylpropan-1-one

DEBT_90_product
Figure 30: DEPT 90 of 2,3-dibromo-3-(4-bromophenyl)-1-phenylpropan-1-one

Appendix #5

IR_spectrum_product
Figure 31: IR spectrum of 3-(4-bromophenyl)-5-phenylisoxazole

NMR_2_product
Figure 32: Proton NMR of 3-(4-bromophenyl)-5-phenylisoxazole

4-bromochalcone
Figure 33: Carbon-13 NMR of 3-(4-bromophenyl)-5-phenylisoxazole

DEPT_45_2_product
Figure 34: DEPT 45 of 3-(4-bromophenyl)-5-phenylisoxazole

DEPT_90_2_product
Figure 35: DEPT 90 of 3-(4-bromophenyl)-5-phenylisoxazole

DEPT_135_2_product
Figure 36: DEPT 135 of 3-(4-bromophenyl)-5-phenylisoxazole

4-bromochalcone
Figure 37: COSY of 3-(4-bromophenyl)-5-phenylisoxazole

HETCOR_product
Figure 38: HETCOR of 3-(4-bromophenyl)-5-phenylisoxazole

Mass_Spec_product
Figure 39: Mass Spectrum of 3-(4-bromophenyl)-5-phenylisoxazole

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